Thermodynamics Research Center / ThermoML | Journal of Chemical and Engineering Data

Solubility of Isoniazid in Supercritical Carbon Dioxide

Heryanto, R.[Rudi], Abdullah, E. C.[Ezzat Chan], Hasan, M.[Masitah]
J. Chem. Eng. Data 2010, 55, 6, 2306-2309
ABSTRACT
Solubility data of isoniazid in supercritical carbon dioxide are important in selecting the most appropriate supercritical methods for pharmaceutical material processing, such as the micronization of isoniazid or the production of isoniazid composites. The solubility of isoniazid in supercritical carbon dioxide was measured using a dynamic analytical method at temperatures of (308, 311, and 313) K and pressures ranging from (13.0 to 18.5) MPa. The result showed that isoniazid solubility increased with the increase of pressure at an isothermal condition and it also increased with the increase of temperature. The experimental data were correlated using the Chrastil and Mendez-Santiago and Teja models. The calculated results show good agreement with the experimental data.
Compounds
# Formula Name
1 C6H7N3O isonicotinic acid hydrazide
2 CO2 carbon dioxide
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • 2
  • Mole fraction - 1 ; Fluid (supercritical or subcritical phases)
  • Temperature, K; Fluid (supercritical or subcritical phases)
  • Pressure, kPa; Fluid (supercritical or subcritical phases)
  • Fluid (supercritical or subcritical phases)
  • Crystal - 1
  • spectrophotometric method
  • 18