Thermodynamics Research Center / ThermoML | Journal of Chemical and Engineering Data

Phase Equilibrium of Biodiesel Compounds for the Triolein + Palmitic Acid + Methanol System with Dimethyl Ether as Cosolvent

Maeda, K.[Kouji], Kuramochi, H.[Hidetoshi], Fujimoto, T.[Taisei], Asakuma, Y.[Yusuke], Fukui, K.[Keisuke], Osako, M.[Masahiro], Nakamura, K.[Kazuo], Sakai, S.-i.[Shin-ichi]
J. Chem. Eng. Data 2008, 53, 4, 973-977
ABSTRACT
In biodiesel production, transesterification in a homogeneous mixture is possible if a solution of triolein and methanol could be prepared with the use of a cosolvent. The volatile solvent dimethyl ether (DME) can make the immiscible mixture of triolein and methanol miscible; moreover, it can be easily recovered due to its high volatility after reaction. Therefore, the vapor liquid liquid equilibrium for the triolein + fatty acid-methanol + DME system was measured by determining the liquid composition, temperature, and pressure of the system. Results showed that DME and palmitic acid effectively promoted the mutual solubilities of triolein and methanol. In addition, the UNIFAC prediction was compared with experimental data, and it was found that the UNIFAC model could represent the complicated phase equilibrium of biodiesel compounds.
Compounds
# Formula Name
1 C57H104O6 1,2,3-tri(cis-9-octadecenoyl)glycerol
2 CH4O methanol
3 C2H6O dimethyl ether
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 2
  • 3
  • 1
  • Vapor or sublimation pressure, kPa ; Liquid mixture 1
  • Mole fraction - 1; Liquid mixture 1
  • Temperature, K; Liquid mixture 1
  • Liquid mixture 1
  • Liquid mixture 2
  • Gas
  • Closed cell (Static) method
  • 13
  • POMD
  • 2
  • 3
  • 1
  • Mole fraction - 2 ; Liquid mixture 1
  • Mole fraction - 1; Liquid mixture 1
  • Temperature, K; Liquid mixture 1
  • Liquid mixture 1
  • Liquid mixture 2
  • Gas
  • synthetic method
  • 13