Thermodynamics Research Center / ThermoML | Journal of Chemical and Engineering Data

Measurement and Correlation of the Solubility of Penicillin V potassium in Ethanol + Water and 1-Butyl alcohol + Water Systems

Wei, T.[Tingting], Wang, C.[Chen], Du, S.[Shichao], Wu, S.[Songgu], Li, J.[Jianyu], Gong, J.[Junbo]
J. Chem. Eng. Data 2015, 60, 1, 112-117
ABSTRACT
The solubility of penicillin V potassium (PVK) in binary ethanol + water and 1-butyl alcohol + water solvent mixtures was measured at temperatures ranging from (278.15 to 313.15) K. The solubility in ethanol + water was measured by a static analytical method while in 1-butyl alcohol + water a dynamic method was adopted. It was found that the solubility of PVK increased with increasing temperature as well as the increase of the initial mole fraction of water. The modified Apelblat equation, the CNIBS/R-K equation, the combined version of the Jouyban-Acree and van t Hoff model, and the hybrid model were used to correlate the solubility data in ethanol + water solvent mixtures, among which the CNIBS/R-K equation gave the best correlation results. The experimental solubility data in 1-butyl alcohol + water were correlated well by the van t Hoff equation and the modified Apelblat equation. The dissolution enthalpy, entropy, and Gibbs energy of PVK in these solvent mixtures were obtained based on the van t Hoff equation.
Compounds
# Formula Name
1 C16H17KN2O5S Penicillin V potassium
2 C2H6O ethanol
3 C4H10O butan-1-ol
4 H2O water
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 2
  • 1
  • 4
  • Mole fraction - 1 ; Liquid
  • Temperature, K; Liquid
  • Solvent: Mole fraction - 2; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • Gravimetric Method
  • 88
  • POMD
  • 3
  • 1
  • 4
  • Mole fraction - 1 ; Liquid
  • Solvent: Mole fraction - 3; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • Gravimetric Method
  • 48