Thermodynamics Research Center / ThermoML | Journal of Chemical and Engineering Data

Measurement and Correlation for Solubility of L-valine in Water, Ethanol, N,N-Dimethylformamide, Acetone, and Isopropyl alcohol between 293.15 and 343.15 K

Zhang, C.[Chuntao], Liu, B.[Bangyu], Wang, x.[xin], Wang, H.[Hairong]
J. Chem. Eng. Data 2014, 59, 9, 2704-2708
ABSTRACT
The solubilities of l-valine in water, ethanol, N,N-dimethylformamide, acetone, and isopropyl alcohol were experimentally measured by the synthetic method over the temperature range from (293.15 to 343.15) K at atmosphere pressure. The solubilities of l-valine in pure solvents increase with increasing temperature and in the following order: acetone less than N,N-dimethylformamide less than isopropyl alcohol less than ethanol less than water. The solubilities correlated using the modified Apelblat model show good agreement with the experimental data, and the dissolution enthalpy, dissolution entropy, and the molar Gibbs energy were predicted. The experimental solubilities and the modified Apelblat model can be used as essential data and model in the industrial manufacturing process of l-valine.
Compounds
# Formula Name
1 C5H11NO2 L-valine
2 C2H6O ethanol
3 C3H6O acetone
4 C3H7NO dimethylformamide
5 C3H8O propan-2-ol
6 H2O water
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • 6
  • Mole fraction - 1 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • laser monitoring
  • 6
  • POMD
  • 2
  • 1
  • Mole fraction - 1 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • laser monitoring
  • 6
  • POMD
  • 5
  • 1
  • Mole fraction - 1 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • laser monitoring
  • 6
  • POMD
  • 4
  • 1
  • Mole fraction - 1 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • laser monitoring
  • 6
  • POMD
  • 3
  • 1
  • Mole fraction - 1 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • laser monitoring
  • 5