Thermodynamics Research Center / ThermoML | Journal of Chemical and Engineering Data

Ternary Liquid Liquid Equilibria of Water + Prop-2-enoic Acid + Isobutyl Ethanoate at Different Temperatures

Zhang, H.[Hongxun], Zhang, Y.[Yingming], Zhang, L.[Lei], Li, C.[Chen], Zhu, C.[Chunshan]
J. Chem. Eng. Data 2011, 56, 8, 3411-3415
ABSTRACT
To screen the proper solvent for separating prop-2-enoic acid aqueous solution by the method of extraction followed by heterogeneous azeotropic distillation, the liquid liquid equilibria (LLE) data for the ternary system water + prop-2-enoic acid + isobutyl ethanoate at (293.15, 303.15, and 313.15) K were measured at atmospheric pressure. The reliability of the experimental LLE data was ascertained through Othmer Tobias and Hand correlations. The LLE phase diagrams at different temperatures for the ternary system were given. Distribution coefficients and separation factors were calculated from the LLE data. The thermodynamic models of nonrandom two-liquid (NRTL) and universal quasichemical activity coefficient (UNIQUAC) were used to correlate the data of the ternay system. The calculated values from both models agree well with the experimental values.
Compounds
# Formula Name
1 C3H4O2 propenoic acid
2 C6H12O2 2-methylpropyl ethanoate
3 H2O water
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • 2
  • 3
  • Mass fraction - 1 ; Liquid mixture 1
  • Mass fraction - 1 ; Liquid mixture 2
  • Mass fraction - 3 ; Liquid mixture 2
  • Temperature, K; Liquid mixture 2
  • Mass fraction - 3; Liquid mixture 1
  • Pressure, kPa; Liquid mixture 2
  • Liquid mixture 1
  • Liquid mixture 2
  • Chromatography
  • Chromatography
  • Chromatography
  • 27