Thermodynamics Research Center / ThermoML | Thermochimica Acta

Thermodynamic study of Ba3CuO4 (s) in Ba-Cu-O system

Mukherjee, Sumanta, Ahamad, Lukman, Dash, S.
Thermochim. Acta 2019, 676, 214-223
ABSTRACT
Ba3CuO4(s) is one of the important compounds as a proton conducting electrolyte which form due to interaction of BaO and CuO. In the present study, Ba3CuO4(s) has been synthesized by solid state route and the Gibbs energy of formation and heat capacity has been experimentally measured by Knudsen Effusion Mass Spectrometer and differential scanning calorimeter. The deltaGf (Ba3CuO4, s, T) and C.deg.p (Ba3CuO4, s, T) is obtained as per given equations: deltaGf (Ba3CuO4, s, T) +- 7 / kJ mol-1 = -1888 + 0.4229.(T / K) C.deg.p (Ba3CuO4, s, T)(J K-1 mol-1) +- 6 = 211 + 0.0274*(T/K) - 3039600.(T /K)-2 The binary phase diagram of BaO-CuO system has been calculated based on the Gibbs energy minimization method. Using the experimental thermodynamic data, isothermal chemical potential diagram of Ba-Cu-C-O system with different axial parameter and ternary phase diagram of Ba (s) - Cu (s) - O2 (g) system has been calculated in order to study the thermodynamic stability and coexisting phases of Ba3CuO4(s).
Compounds
# Formula Name
1 CBaO3 barium carbonate
2 CuO copper(II) oxide
3 CO2 carbon dioxide
4 Ba3CuO4 barium copper oxide (Ba3CuO4)
5 BaO barium oxide (BaO)
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 4
  • Mass density, kg/m3 ; Crystal
  • Temperature, K; Crystal
  • Pressure, kPa; Crystal
  • Crystal
  • X-ray diffraction
  • 1
  • POMD
  • 4
  • Molar heat capacity at constant pressure, J/K/mol ; Crystal
  • Temperature, K; Crystal
  • Pressure, kPa; Crystal
  • Crystal
  • DSC
  • 27
  • POMD
  • 2
  • Molar heat capacity at constant pressure, J/K/mol ; Crystal
  • Temperature, K; Crystal
  • Pressure, kPa; Crystal
  • Crystal
  • DSC
  • 22
  • POMD
  • 5
  • Molar heat capacity at constant pressure, J/K/mol ; Crystal
  • Temperature, K; Crystal
  • Pressure, kPa; Crystal
  • Crystal
  • DSC
  • 22
  • RXND
  • 1
  • 2
  • 4
  • 3
  • Molar Gibbs energy of reaction, kJ/mol
  • Quadruple mass spectroscopy
  • 16