Thermodynamics Research Center / ThermoML | Journal of Chemical Thermodynamics

Comprehensive thermophysical and thermochemical studies of vanillyl alcohol

Freitas, V. L. S.[Vera L. S.], Lima, A. C. M. O.[Ana C. M. O.], Sapei, E.[Erlin], Ribeiro da Silva, M. D. M. C.[Maria D. M. C.]
J. Chem. Thermodyn. 2016, 102, 287-292
ABSTRACT
In this work, energetic and structural studies concerning vanillyl alcohol, based both on experimental and computational studies, were developed. The massic energy of combustion and the vapour pressures at different temperatures were measured by static bomb combustion calorimetry and Knudsen mass-loss effusion techniques, respectively. The computational studies were performed using the G3(MP2)//B3LYP method. The combination of experimental and computational data enabled the determination of the enthalpies, entropies and Gibbs energies of sublimation and formation of this compound both in the crystal and gas phase. The intramolecular hydrogen bond energy present in vanillyl alcohol was evaluated, together with the O H homolytic bond dissociation enthalpy. The new data are very useful for process design and development in the biorefinery.
Compounds
# Formula Name
1 CO2 carbon dioxide
2 H2O water
3 O2 oxygen
4 C8H10O3 4-hydroxy-3-methoxybenzyl alcohol
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 4
  • Vapor or sublimation pressure, kPa ; Crystal
  • Temperature, K; Crystal
  • Crystal
  • Gas
  • Calculated from knudsen effusion weight loss
  • 30
  • RXND
  • 4
  • 1
  • 2
  • 3
  • Specific internal energy of reaction at constant volume, J/g
  • Static bomb calorimetry
  • 1