Thermodynamics Research Center / ThermoML | Journal of Chemical Thermodynamics

Solubilities of betulin and betulinic acid in sodium hydroxide aqueous solutions of varied mole fraction at temperatures from 283.2 K to 323.2 K

Fan, J.-P.[Jie-Ping], Xie, C.-F.[Chun-Fang], Luo, Y.-S.[Yun-Song], Song, F.-t.[Fa-tian], Liu, X.-Y.[Xiao-Ying], Zhu, J.-H.[Jian-Hang], Zhang, X.-H.[Xue-Hong]
J. Chem. Thermodyn. 2013, 67, 1-4
ABSTRACT
The solubilities of betulin and betulinic acid were measured at varied values of mole fraction of sodium hydroxide aqueous solutions at a series of temperature (283.2, 293.2, 303.2, 313.2, and 323.2) K. They increase with the increase of temperature. Furthermore, the solubility of betulinic acid has a positive correlation with the mole fraction of sodium hydroxide aqueous solutions, and so is that of the betulin. The experimental solubility resuls are well correlated by the modified Apelblat equation. The enthalpy and entropy of betulin and betulinic acid during the dissolution process in sodium hydroxide aqueous solutions are calculated with the van't Hoff equation. The results indicate that the dissolution process is endothermal reaction that is driven by entropy.
Compounds
# Formula Name
1 C30H50O2 betulin
2 C30H48O3 betulinic acid
3 HNaO sodium hydroxide
4 H2O water
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • 3
  • 4
  • Mole fraction - 1 ; Liquid
  • Solvent: Mole fraction - 3; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • Chromatography
  • 25
  • POMD
  • 2
  • 3
  • 4
  • Mole fraction - 2 ; Liquid
  • Solvent: Mole fraction - 3; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 2
  • Chromatography
  • 25