Thermodynamics Research Center / ThermoML | Journal of Chemical Thermodynamics

Advanced calibration, adjustment, and operation of a density and sound speed analyzer

Fortin, T. J.[Tara J.], Laesecke, A.[Arno], Freund, M.[Malte], Outcalt, S.[Stephanie]
J. Chem. Thermodyn. 2013, 57, 276-285
ABSTRACT
Benchtop measurement systems have emerged as powerful tools in the ongoing quest for thermophysical property data. We demonstrate that these instruments can yield results of high quality if operated in an informed manner. The importance of sample purity, reproducibility over repeatability, expanded calibration and adjustment protocols, and rigorous uncertainty estimates are emphasized. We report measurement results at ambient atmospheric pressure and temperatures from 343 K to 278 K, including expanded uncertainty estimates, for the density and speed of sound of isooctane and for the speed of sound of toluene. These data are useful for validating the performance of such instruments.
Compounds
# Formula Name
1 C7H8 toluene
2 C8H18 2,2,4-trimethylpentane
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • Speed of sound, m/s ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Sing-around technique in a fixed-path interferometer
  • 14
  • POMD
  • 2
  • Mass density, kg/m3 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • VIBTUB:mpoint
  • 14
  • POMD
  • 2
  • Speed of sound, m/s ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Sing-around technique in a fixed-path interferometer
  • 14