Thermodynamics Research Center / ThermoML | Journal of Chemical Thermodynamics

Renewable platform-chemicals and materials: Thermochemical study of levulinic acid

Verevkin, S. P.[Sergey P.], Emelyanenko, V. N.[Vladimir N.]
J. Chem. Thermodyn. 2012, 46, 94-98
ABSTRACT
The standard molar enthalpy of formation in the gaseous state (-613.5 +- 2.2) kJ mol-1 of levulinic acid has been obtained from combustion calorimetry and results from the temperature dependence of the vapour pressure measured by the transpiration method. In order to verify the experimental data, firstprinciples calculations have been performed. Enthalpies of formation derived from G4 and G3MP2 methods are in an excellent agreement with the experimental results. Thermodynamic analysis of the hydrolysis of 5-hydroxymethylfurfural to the levulinic and formic acids has revealed very high feasibility of these reactions with equilibrium constants completely shifted to the desired reaction products even at T = 298.15 K.
Compounds
# Formula Name
1 CO2 carbon dioxide
2 H2O water
3 O2 oxygen
4 C5H8O3 4-oxopentanoic acid
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 4
  • Molar enthalpy of vaporization or sublimation, kJ/mol ; Liquid
  • Temperature, K; Liquid
  • Liquid
  • Gas
  • Derived by Second law
  • 1
  • POMD
  • 4
  • Vapor or sublimation pressure, kPa ; Liquid
  • Temperature, K; Liquid
  • Liquid
  • Gas
  • Transpiration method
  • 12
  • RXND
  • 4
  • 1
  • 2
  • 3
  • Specific internal energy of reaction at constant volume, J/g
  • Static bomb calorimetry
  • 1