Thermodynamics Research Center / ThermoML | Journal of Chemical Thermodynamics

Thermodynamic properties of caffeine: Reconciliation of available experimental data

Emelyanenko, V. N.[Vladimir N.], Verevkin, S. P.[Sergey P.]
J. Chem. Thermodyn. 2008, 40, 12, 1661-1665
ABSTRACT
Molar enthalpies of sublimation of two crystal forms of caffeine were obtained from the temperature dependence of the vapour pressure measured by the transpiration method. A large number of primary experimental results on the temperature dependences of vapour pressure and phase transitions have been collected from the literature and have been treated in a uniform manner in order to derive sublimation enthalpies of caffeine at T = 298.15 K. This collection together with the new experimental results reported here has helped to resolve contradictions in the available sublimation enthalpies data and to recommend a consistent and reliable set of sublimation and formation enthalpies for both crystal forms under study. Ab initio calculations of the gaseous molar enthalpy of formation of caffeine have been performed using the G3MP2 method and the results are in excellent agreement with the selected experimental data.
Compounds
# Formula Name
1 C8H10N4O2 caffeine
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • Vapor or sublimation pressure, kPa ; Crystal 2
  • Temperature, K; Crystal 2
  • Crystal 2
  • Gas
  • Transpiration method
  • 12
  • POMD
  • 1
  • Vapor or sublimation pressure, kPa ; Crystal 1
  • Temperature, K; Crystal 1
  • Crystal 1
  • Gas
  • Transpiration method
  • 4