Thermodynamics Research Center / ThermoML | Journal of Chemical Thermodynamics

Thermochemical studies of 3-methylpyrazole and 1,3,5-trimethylpyrazole

Ribeiro da Silva, M. A. V.[Manuel A. V.], Figueiredo, D. F.[Diogo F.], Cabral, J. I. T. A.[Joana I. T. A.]
J. Chem. Thermodyn. 2008, 40, 3, 369-374
ABSTRACT
The standard op 1/4 0:1 MPaP molar enthalpies of formation, at T 1/4 298:15 K, in the condensed phases of two alkylpyrazoles, viz. 3-methylpyrazole and 1,3,5-trimethylpyrazole, were determined by static bomb calorimetry. Calvet microcalorimetry was used to measure the standard molar enthalpy of vaporisation of 1-methylpyrazole and the standard molar enthalpy of sublimation of 1,3, 5-trimethylpyrazole. From these two sets of results, the standard molar enthalpies of formation of both alkylpyrazoles in gaseous phase, at T 1/4 298:15 K, were derived. The final results were analysed and discussed in terms of molecular structure.
Compounds
# Formula Name
1 CO2 carbon dioxide
2 N2 nitrogen
3 H2O water
4 O2 oxygen
5 C4H6N2 3-methylpyrazole
6 C6H10N2 1,3,5-trimethylpyrazole
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 5
  • Molar enthalpy of transition or fusion, kJ/mol ; Liquid
  • Temperature, K; Liquid
  • Liquid
  • Gas
  • Calvet calorimetry with correction to 298 K for gas heat capacity
  • 1
  • POMD
  • 6
  • Molar enthalpy of transition or fusion, kJ/mol ; Crystal
  • Temperature, K; Crystal
  • Crystal
  • Gas
  • Calvet calorimetry with correction to 298 K for gas heat capacity
  • 1
  • RXND
  • 5
  • 1
  • 2
  • 3
  • 4
  • Specific internal energy of reaction at constant volume, J/g
  • Static bomb calorimetry
  • 1
  • RXND
  • 6
  • 1
  • 2
  • 3
  • 4
  • Specific internal energy of reaction at constant volume, J/g
  • Static bomb calorimetry
  • 1