Thermodynamics Research Center / ThermoML | Fluid Phase Equilibria

Solubility of naproxen in ethyl acetate + ethanol mixtures at several temperatures and correlation with the Jouyban-Acree model

Rodriguez, G. A., Delgado, D. R.[Daniel R.], Martinez, F.[Fleming], Jouyban, A.[Abolghasem], Acree, Jr., W. E.[William E.]
Fluid Phase Equilib. 2012, 320, 49-55
ABSTRACT
By using the van't Hoff and Gibbs equations the thermodynamic functions Gibbs energy, enthalpy, and entropy of solution and of mixing of naproxen (NAP) in some ethyl acetate + ethanol mixtures were evaluated from solubility data determined at several temperatures. By means of enthalpy-entropy compensation analysis, a non linear delta_H vs. delta_G compensation plot with negative and positive slopes was obtained if all the composition intervals are considered. Finally, the Jouyban-Acree model has been applied to correlate the drug solubilities as well as the respective thermodynamic quantities of solution in these solvent mixtures.
Compounds
# Formula Name
1 C14H14O3 (S)-(+)-naproxen
2 C4H8O2 ethyl acetate
3 C2H6O ethanol
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 3
  • 2
  • 1
  • Mole fraction - 1 ; Liquid
  • Temperature, K; Liquid
  • Solvent: Mass fraction - 2; Liquid
  • Pressure, kPa; Liquid
  • Liquid
  • Crystal - 1
  • Gravimetric
  • 55