Thermodynamics Research Center / ThermoML | Fluid Phase Equilibria

Solubility of CF4 in lower alcohols

Sousa, J. M. M. V., Ferreira, A. G. M., Fachada, H. C., Fonseca, I. M. A.
Fluid Phase Equilib. 2010, 296, 2, 95-98
ABSTRACT
This work is inserted in a research program that consists mainly in the experimental and theoretical study of the effect of association/solvation between solute and solvent molecules in the solubility of gases in liquids. The solubilities of tetrafluoromethane in lower alcohols (methanol, ethanol, 1-propanol, 1-butanol) have been determined in the temperature range of 288-308 K, at atmospheric pressure, using an automated apparatus recently assembled in our laboratory. An accuracy of 0.6 % and a precision of the same order of magnitude was achieved. The solubility is the lowest in methanol which is the highest associated alcohol and increases with the C-content of the alcohol. The molar Gibbs energy, enthalpy and entropy of solution were calculated from the experimental results (at 1 atm partial pressure of the gas and 298 K). A semiempirical correlation between the solubility of CF4 in alcohols at 298 K and the Gutmann acceptor number (AN) of the solvents has been developed.
Compounds
# Formula Name
1 CH4O methanol
2 CF4 tetrafluoromethane
3 C2H6O ethanol
4 C3H8O propan-1-ol
5 C4H10O butan-1-ol
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • 2
  • Mole fraction - 2 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa - 2; Gas
  • Liquid
  • Gas
  • Volumetric method
  • 9
  • POMD
  • 3
  • 2
  • Mole fraction - 2 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa - 2; Gas
  • Liquid
  • Gas
  • Volumetric method
  • 9
  • POMD
  • 4
  • 2
  • Mole fraction - 2 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa - 2; Gas
  • Liquid
  • Gas
  • Volumetric method
  • 9
  • POMD
  • 5
  • 2
  • Mole fraction - 2 ; Liquid
  • Temperature, K; Liquid
  • Pressure, kPa - 2; Gas
  • Liquid
  • Gas
  • Volumetric method
  • 9