Thermodynamics Research Center / ThermoML | International Journal of Thermophysics

A Capillary Tube Viscometer Designed for Measurements of Hydrogen Gas Viscosity at High Pressure and High Temperature

Yusibani, E.[Elin], Nagahama, Y.[Yosuke], Kohno, M.[Masamichi], Takata, Y.[Yasuyuki], Woodfield, P.[Peter], Shinzato, K.[Kanei], Fujii, M.[Motoo]
Int. J. Thermophys. 2011, 32, 6, 1111-1124
ABSTRACT
A capillary tube viscometer was developed to measure the dynamic viscosity of gases for high pressure and high temperature. The apparatus is simple and designed for safe-handling operation. The gas was supplied to the capillary tube from a high-pressure reservoir tank through a pressure regulator unit to maintain a steady state flow. The measurements of a pressure drop across the capillary tube with high accuracy under extreme conditions are the main challenge for this method. A differential pressure sensor for high pressures up to 100 MPa is not available commercially. Therefore, a pair of accurate absolute pressure transducers was used as a differential pressure sensor. Then the pressure drop was calculated by subtracting the outlet pressure from the inlet one with a resolution of 100 Pa at 100 MPa. The accuracy of the present measurement system is confirmed by measuring the viscosity of nitrogen as a reference gas. The apparatus provided viscosities of nitrogen from ambient temperature to 500 K and hydrogen from ambient temperature to 400 K and for pressures up to 100 MPa with a maximum deviation of 2.2 % compared with a correlation developed by the present authors and with REFPROP (NIST).
Compounds
# Formula Name
1 N2 nitrogen
2 H2 hydrogen
Datasets
The table above is generated from the ThermoML associated json file (link above). POMD and RXND refer to PureOrMixture and Reaction Datasets. The compound numbers are included in properties, variables, and phases, if specificied; the numbers refer to the table of compounds on the left.
Type Compound-# Property Variable Constraint Phase Method #Points
  • POMD
  • 1
  • Viscosity, Pa*s ; Gas
  • Temperature, K; Gas
  • Pressure, kPa; Gas
  • Gas
  • Capillary tube (Ostwald; Ubbelohde) method
  • 32
  • POMD
  • 2
  • Viscosity, Pa*s ; Gas
  • Temperature, K; Gas
  • Pressure, kPa; Gas
  • Gas
  • Capillary tube (Ostwald; Ubbelohde) method
  • 17